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Cikakken jini biyar abubuwa analyzer
Bayanin Amfani da Binciken Binciken Binciken Binciken Binciken Binciken Binciken Binciken Binciken Binciken Binciken Binciken Binciken Binciken Bincik
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Biyar abubuwa analyzer amfani da umarnin
1 Bayani
1.1 Amfani
Ana amfani da abubuwa biyar a cikin cikakken jinin mutum (ƙididdigar calcium jan ƙarfe magnesium baƙin ƙarfe zinc).
1.2 Tsarin
FEA jini biyar abubuwa analyzer ya kunshi da masauki, kwamfuta tsarin, firintar, iska iska tushen, acetylene ** na'urar da acetylene kwalba da sauransu. Duba hoto na 1.2. FEA jini biyar abubuwa analyzer ne m optical bincike kayan aiki.
1.5 Ka'idar aiki
A tushen halin atom a cikin wuta sha biyar abubuwa hollow cathode fitilar fitar da biyar resonance layi, bayan da concave grating da kuma mayar da hankali tasiri bisa ga grating equation sa resonance layi mayar da hankali a kan wani gap a kan Roland zagaye, haskaka a kan biyar photoelectric bututun. Saita mummunan high ƙarfin lantarki na fitila halin yanzu da photoelectric multiplier bututun sa haske ** watsawa zuwa 99.9%. Ma'auna abun ciki na abubuwa bisa ga sha na atom na layin resonance.
C = c × A × A + b × A + a
A - tsananin;
A, b, c daidaituwa;
C - matattarar abubuwan da za a auna;
1.6 Babban fasali
1.6.2 Ajiye ** lokaci, biyar abubuwa hada zuwa wani m samar da cathode fitila, biyar abubuwa a lokaci guda **, wannan kayan aiki iya daidaitawa auna abun ciki na jan ƙarfe, zinc, calcium, magnesium, baƙin ƙarfe biyar abubuwa a cikin dakika 10. Daidai da sauri.
1.6.3 amfani da keɓaɓɓun reagents, watsa da rikitarwa pre-processing tsari ga samfurin, rage gurɓataccen hali ga samfurin da * ma'aikata, tabbatar da daidaito na ** bayanai;
1.6.3 tabbatar da girman gas (C2H2) kwarara na ƙonewa mai amfani da rabo, don haka ƙonewa mai amfani da rabo ba zai canza a kowane lokacin da mai bincike ya fara;
1.6.4 Fixed wuta height matsayi, sa kowane ma'auni da daidai data;
1.6.5 musamman optical hanyar zane, ta amfani da hadewa fitila rack, tabbatar da fitila aiki matsayi, kawar da analyst aiki na daidaita fitila matsayi, sa ma'auni mafi m da daidai;
1.6.6 Wannan kayan aiki ne sanye da universal microcomputer, gudanar da FEA software, zai iya samun atomatik iko a kan baƙi, zai iya nuna daban-daban data da kuma nazarin curves a kan nuni, kuma yana da buga, ajiya, kira da kuma sake sarrafa aiki a kan nazarin sakamakon.
1.6 Babban fasaha nuna alama
1.6.1 ** Nau'in: I Class, B Type;
1.6.2 aiki tsari: tsakanin lokaci loading, ci gaba da aiki;
1.6.3 Shigar da ikon: 300VA;
1.6.4 narkewa waya model: 3A / 250V (Φ5mm × 20mm);
1.6.5 Yawan spectrum tashoshi: biyar tashoshi;
1.6.6 monochrome mai: Holographic grating monochrome mai ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin ƙarancin;
1.6.7 absorption kewayon: 0 ~ 2Abs;
1.6.8 wuta atomizer: Pre-haɗuwa irin guda suture mai ƙona;
1.6.9 hanyar aunawa: Abs (absorption) da kuma mayar da hankali. Number karantawa hanyar: lokaci darajar, peak yanki darajar;
1.6.10 aikin aiki: atomatik daidaitawa sifili, samfurin maimaita ma'auni, samfurin maimaita ma'auni;
1.6.11 sakamakon kididdiga ayyuka: Matsakaicin, SD (misali karkatarwa) da RSD (dangane da misali karkatarwa);
1.6.12 ta atomatik kashe acetylene, ** ta atomatik kashe lokacin da iska matsin lamba kasa da 0.15MPa;
1.6.13 tare da atomatik saita mummunan matsin lamba, atomatik daidaitawa sifili iko, atomatik makamashi daidaitawa, kwamfuta nuni da kuma buga aiki;
1.6.14 daidaitaccen ma'auni: daya ci gaba, daidaitaccen ma'auni abun ciki na jan ƙarfe, zinc, calcium, magnesium, baƙin ƙarfe biyar a cikin dakika 10.
1.7 Performance nuna alama (kamar rubutaccen sabon gwaji fayil)
Abubuwan calcium Ca jan ƙarfe Cu magnesium Mg baƙin ƙarfe Fe zinc Zn
Yanzu haske ƙarfin lantarki% <0.5% <0.5% <0.5% <0.5% <0.5% <0.5%
tushen layin amo fadi < ± 0,006 < ± 0,006 < ± 0,006 < ± 0,006 < ± 0,006
Kuskuren layi% <6 <6 <6 <6 <6
ƙwarewa A > 0.1 > 0.05 > 0.1 > 0.1 > 0.1
Absorption dangantaka karkatarwa% <5 <5 <5 <5 <5
Gano iyaka mg / L <0.1 <0.1 <0.8 <0.1
siffofin mayar da hankali mg / L <0,06 <0,06 <0,06 <0,7 <0,06
2 Kayan aiki Shigarwa & Acceptance
2.1 kayan aiki * da ake bukata
2.1.1 dakin yanayin zafin jiki 5 ℃ ~ 35 ℃;
2.1.2 dakin gwaje-gwaje dangi zafi ba fiye da 75%;
2.1.3 rawar jiki da kuma electromagnetic tsangwama da dakin gwaje-gwaje ba tasiri kayan aiki amfani;
2.1.4 dakin gwaje-gwaje ya kamata a raba daga dakin gwaje-gwaje na sunadarai don hana ganowa da kuma daidaito na'ura sassa na acid, alkali da sauran lalata gas ko hayaki lalata kayan aiki.
2.1.5 dakin gwaje-gwaje ya kamata ya kasance mai tsabta, bushewa da ƙura. A cikin gida babu lalata gas, da kyau iska na'urori;
2.1.6 da dakin gwaje-gwaje aiki tebur ya kamata ya daidaita da karfi, bayan sanya kayan aiki ba deformation. Akwai isasshen sarari a kusa da haɗin kewayawa, hanyoyin iska da kayan aikin gyara don sauƙin gyara.
2.1.7 samar da wutar lantarki: AC ƙarfin lantarki 220V ± 22V, mitar 50Hz ± 1Hz. Kayan aiki dole ne su sami kyakkyawan haɗi, gabaɗaya haɗi juriya < 0.1Ω;
2.1.8 Gas tushen yanayi:
Air: mai-free iska kwamfuta: 0.23MPa matsin lamba; Nominal girman kwarara: 0.3m3 / h ~ 0.9m3 / h;
Acetylene: Yawancin lokaci ya kamata a yi amfani da karfe kwalba tsabtace acetylene, tsabtace fiye da 99%. Acetylene karfe kwalbar ya kamata a sanya a cikin wani mai kyau iska, ba tare da ruwan sama da kuma rana kai tsaye, da muhalli zafin jiki ya kamata kasa da 35 ° C, kuma ya kamata a yi nisa da lantarki rarraba kwamfuta, high karfin wutar lantarki samar da, layi da kuma mai ƙonewa, fashewa abubuwa. Ya kamata a sami alamar wuta ta ** a wurin da aka sanya, kuma ya kamata a yi amfani da masu kashe wuta. Gas amfani da ** Sauran matsin lamba ba kasa da 0.4MPa;
2.1.9 Kwamfuta mai karɓar baƙi (kayan haɗi na zaɓi): Microcomputer tsarin da ke sama da CPU200MHz. Nuni pixel saiti: 1280 × 768; da kuma saita printer da ya dace da shi;
2.1.10 misali jerin mafita da kuma misali reagents samar da masana'antun;
2.1.11 Mai ƙonewa mai wuta.
2.2 Kayan aiki Shigarwa
FEA jini biyar abubuwa analyzer haɗi da daban-daban sassa, don haɗi daidai da zane-zane a Figure 1.4. Takaddun matakai kamar waɗannan:
2.2.1 A shirye don samar da wutar lantarki plugs tare da uku saiti na uku jacks, duba aiki wutar lantarki ta wutar lantarki tare da Multimeter, don saduwa da amfani da bukatun;
2.2.2 haɗa kwamfuta tare da FEA biyar abubuwa jini analyzer ta hanyar 232 serial tashar;
2.2.3 Haɗa kwamfutarka da firintar kuma yi gwajin bugawa.
2.2.4 Haɗa iska kwamfuta tare da FEA biyar abubuwa jini analyzer, haɗi ta amfani da roba bututun, da kuma tighten tare da karfe tufafi, lura da haɗi da iska kwamfuta na drainage bututun da ƙasa gida drainage;
2.2.5 An haɗa kwalban acetylene mai tsarkakewa tare da mai sarrafa acetylene, sa'an nan kuma an haɗa mai sarrafa acetylene zuwa mai nazarin jini na FEA biyar;
2.2.6 A kasa karshen atomizer da sharar ruwa bakin, sharar ruwa bakin yana da tsawon kimanin mita 1.5 na sharar ruwa bututun, don kawar da sharar ruwa, a tsakiyar bututun da kewaye da daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitaccen daidaitac Saka kashin karshen bututun ruwa a cikin kwandon roba ko kwalban gilashi, kada ku saka bututun ruwa a ƙasa da ruwan ruwa ko kai tsaye a cikin tsarin ruwa na dakin gwaje-gwaje.
Lura: dole ne a duba ruwa a cikin hatimi har zuwa *** engraving line kafin ƙonewa.
2.2.7 Bude iska kwamfuta daidaitawa zuwa aiki matsin lamba, sa'an nan kuma bude iska shiga bawul na FEA biyar abubuwa jini analyzer, duba hatimi na haɗi maki tare da sabulu ruwa;
2.2.8 bude acetylene karfe kwalba, daidaita zuwa al'ada aiki matsin lamba, bude acetylene mai kula da kuma hura acetylene wuta, duba hatimi na waje iska hanyar haɗin da ruwa, da kayan aiki zai atomatik ** idan akwai zubuwa a cikin kayan aiki;
2.2.9 Gas hanyar da aka kashe duk bayan al'ada, bude kwamfuta da kuma FEA biyar abubuwa jini analyzer ikon, duba ko kayan aiki ya wuce da al'ada;
2.3 Karɓar kayan aiki
2.3.1 Cikakken samfurin karɓa
Binciken cikakkiyar kowane ɓangare na samfurin bisa ga dubawa na ɗaya;
2.3.2 Samfurin aikin karɓa
Bincike a kan software shigarwa a babi na 3 da kuma gwajin a babi na 4 * jagora don cimma bukatun kayan aiki aikin nuna alama da aka tsara a 1.7.
3 Software na FEA
3.1 Saitunan ƙuduri na nuni
Saitunan ƙuduri na nuni: 1280 × 768, duba Hoto 3.1.
3.2 Shigarwa da software
A karkashin tsarin Windows *, kwafe FEA matsa software a kan * D disk, unzip zuwa fayil ɗin yanzu (X).
3.3 Fara FEA biyar abubuwa analyzer tsarin
Double danna FEA icon a kan tebur na WINDOWS
Yanzu shiga shafin farko na FEA Five Element Analyzer * don dubawa. Duba Hoto 3.3.1. Idan software ba zai iya aiki yadda ya kamata ba, shi zai iya aiki yadda ya kamata bayan shigar da VB6.
Yanzu shiga shafin farko na FEA Five Element Analyzer * don dubawa. Duba Hoto 3.3.1. Idan software ba zai iya aiki yadda ya kamata ba, shi zai iya aiki yadda ya kamata bayan shigar da VB6.
4 Kayan aiki yanayin saiti
Danna "1 kayan aiki yanayin" katin don shiga kayan aiki saitunan dubawa, duba Figure 4.0.
4.1 Saitunan tashar sadarwa ta COM
Danna kayan aiki yanayin katin, danna COM tashar sadarwa single-zaɓi button don zaɓar tashar sadarwa, danna
Buttons don adana lambar kalmar sadarwa, duba Figure 4.1.
Buttons don adana lambar kalmar sadarwa, duba Figure 4.1.
4.2 Samfurin hanyoyin thinning
40 microliters jini samfurin aka ƙara * 1.00ml jini samfurin diluent. Duba hoto 4.2.
4.3 Daidaito
Daidaito yana nuna daidaito na sakamakon ma'auni. Duba hoto na 4.2.
4.4 daidaitattun daidaitawa saiti
Dangantaka tsakanin jerin lambobi da mayar da hankali duba Figure 4.4. FEA biyar abubuwa analyzer amfani da misali aiki curve quantitative.
An ƙara samfurin jini na 40μL a cikin * 1000μL diluent. (1+0.040) / 0.04 = 26 sau
Hoto 4.4 daidaitattun daidaitawa saiti
4.5 Zaɓin abubuwa
Abubuwan da aka zaɓa za a iya nuna sakamakon ** a cikin buga rahotanni da buga kwaikwayo. Duba hoto na 4.5. Lokacin da calcium spectrum farko shiga suture, saita calcium daya abu auna.
4.6 Ma'auni darajar kewayon saiti
Unit na sakamakon ma'auni na abubuwa a cikin jini duba Figure 4.6. Sakamakon auna abubuwan da ke cikin jini ya kamata ya kasance a cikin iyakar sama da ƙasa.
Alamar sama da ƙasa zaɓi "Yes", sa'an nan alamun "↓" da "↑" suna nunawa a lokacin ma'auni.
Alamar sama da ƙasa zaɓi "A'a", don haka ba a nuna alamun "↓" da "↑" yayin aunawa ba, kawai ƙimar aunawa.
4.7 Rahoton gaba
Yayin buga rahoton, buga "sunan asibiti", "Mai binciken likita", "Mai binciken likita", "Binciken asibiti", da kuma "Bayanan kula". Duba hoto 4.7.
5 auna biyar abubuwa a cikin jini (ci gaba da samfurin)
5.1 Shiga zuwa auna dubawa: Duba Figure 5.1.
5.2 Lighting halin yanzu saiti da T100 watsawa saiti
5.2.1 Saitunan yanzu na haske: danna
button, saita fitila yanzu 5mA; danna ↓ button don rage hasken yanzu; Danna ↑ button don rage hasken yanzu. Duba hoto na 5.1.
button, saita fitila yanzu 5mA; danna ↓ button don rage hasken yanzu; Danna ↑ button don rage hasken yanzu. Duba hoto na 5.1.5.2.2 Saitunan watsawa T100: danna
Button, ta atomatik kammala mummunan high karfin ƙarfi saiti da ake buƙata don haske transmittance T na 5 photoelectric multiplier bututun ya kai 99.9%. Idan watsawa ba zai iya kai 99.9%, sake danna maɓallin don sa T ya kai 99.9%. Wannan tsari shine aiwatar da daidaitawar makamashi ta atomatik ga bututun lantarki.
Button, ta atomatik kammala mummunan high karfin ƙarfi saiti da ake buƙata don haske transmittance T na 5 photoelectric multiplier bututun ya kai 99.9%. Idan watsawa ba zai iya kai 99.9%, sake danna maɓallin don sa T ya kai 99.9%. Wannan tsari shine aiwatar da daidaitawar makamashi ta atomatik ga bututun lantarki.5.3 Ma'auni Total lokaci da kuma ma'auni samfurin tsakanin lokaci
Ma'auni Total lokaci = Ma'auni samfurin tsakanin lokaci × 1 + misali samfurin adadin + samfurin adadin)
Figure 5.3 Ma'auni samfurin lokaci
5.4 Shirya daidaitaccen jerin mafita: Bude rufin kwalba don daidaitaccen bayani na 0, buɗe rufin kwalba don daidaitaccen bayani na 1, buɗe rufin kwalba don daidaitaccen bayani na 2, buɗe rufin kwalba don daidaitaccen bayani na 3.
5.5 Samun jini da kuma shirya samfurin jini
Taka 40 microliters ba tare da coagulation ƙarshen jini samfurin, da sauri kara * 1ml cikakken jini biyar abubuwa ** reagent centrifugal roba bututun, da kuma hada-hada anti-coagulation.
5.6 ƙonewa
5.6.1 Tabbatar da cewa iska hanyar haɗi ne mai kyau, daidaita kwararar daidaitawa bawul na iska kwamfuta a saba da agogo zuwa **, bude iska kwamfuta ikon samarwa, daidaita kwararar bawul a saba da agogo, sa iska matsin lamba ne 0.23Mpa.
5.6.2 Bude bawul na acetylene karfe kwalba, daidaita biyu matsin lamba mita, tabbatar da cewa acetylene matsin lamba ne 0.03Mpa.
5.6.3 A kan bude acetylene ** na'urar wutar lantarki, danna [** button] a lokaci guda kunna ƙonawa kai da wuta lighter.
5.6.4 daidaita acetylene kusa da ƙonawa kai tare da iska iko bawul, lura da wuta kwanciyar hankali, da launi ne a tanned dakatar. Ma'auni suction hakkin kimanin 6ml / min.
5.6.5 Bayan ƙonewa dole ne a lura da wuta na biyu biyu biyu biyu, idan wuta ta kashe ba zato ba tsammani saboda tsawon bututun acetylene ko rashin kwanciyar hankali na matsin lamba, lokacin da aka gano wuta ta kashe ba zato ba tsammani, don Allah kashe mai kula da acetylene nan da nan.
5.6.6 Don amfani da **, wannan samfurin yana sarrafa gas na acetylene ta hanyar mai sarrafa acetylene daban-daban, idan kashewa ba zato ba tsammani ya faru, za a iya kashe mai sarrafa acetylene kai tsaye. Idan kana buƙatar sake ƙonewa, sai ka kunna wuta ta hanyar ƙonewa.
5.7 daidaitawa T = 100
Danna button, jira game da 10 seconds, watsa haske ya kai 95% ~ 105 kewayon, danna
Button ƙarshe.
Button ƙarshe.5.8 Ma'auni ** mafita, misali mafita da samfurin mafita
Lokaci matsayi na rawaya frame ** shine karatu na absorbance ** maki, a lokacin da aka auna ya kamata a sanya kwanciyar hankali na absorbance a cikin rawaya frame ***.
suction kai a cikin ruwa distilled, danna
A cikin "auna" button, wadannan tips bayyana:
A cikin "auna" button, wadannan tips bayyana:
5.9 absorption na karɓar ** mafita, misali mafita da samfurin mafita daga stationary spectrography
Canja wurin duk daidaitaccen absorption: danna kan "Canja wurin absorption" button don canja wurin duk ** bayani, daidaitaccen bayani, da kuma samfurin bayani na absorption * a cikin tebur a kan spectrogram ta atomatik.
5.10 daidaitattun lissafi
Danna "Nuna daidaitaccen aiki curve" button a cikin toolbar, da kuma bayanai a cikin dawowa lissafin nazarin lissafi tebur nuna, idan kana so ka duba daidaitaccen aiki curve, danna button a daidaitaccen absorption ma'auni tebur. Duba hoto 5.10.
5.12 Abubuwan da ke ciki Unit Converter umarnin:
1.00mg / L na calcium = 1 / 40.08 mmol / L na calcium = 0.02495 mmol / L na calcium = K1
1.00mg / L baƙin ƙarfe = 1 / 55.847 mmol / L baƙin ƙarfe = 0.017906 mmol / L baƙin ƙarfe = K2
1.00mg / L jan ƙarfe = 1000 / 63.546 μmol / L jan ƙarfe = 15.7366 μmol / L jan ƙarfe = K3
1.00mg / Lmagnesium = 1 / 24.305 mmol / Lmagnesium = 0.041144 mmol / Lmagnesium = K4
1.00mg / L zinc = 1000 / 65.38 μmol / L zinc = 15.295 μmol / L zinc = K5
5.13 Abubuwan da ke ciki lissafi formula
Cikakken ion a cikin samfurin jini Cx = Ci × Ki × (1.0 + 0.040) / 0.040
Tsarin:
Cx - matakan ion a cikin samfurin jini;
Ci - matattarar ion a cikin samfurin da aka gwada, mg/L；
1.0 - girman diluent, mL；
0.04 — girman samfurin jini, mL。
(1.0+0.040) /0.040 = 26
5.14 Samfurin rahoto
Danna 3 Samfurin rahoto katin don buga samfurin rahoto.
5.14.1 Shirya rahoto sigogi
Rubuta sunan, jinsi, shekaru, aikace-aikace lambar, tarihin likita lambar, asibitin asibiti lambar, gado lambar, samfurin sunan, aikawa lokaci, rahoto lokaci a cikin samfurin rahoto sigogi tebur. Duba hoto na 6.15.
5.14.2 Nuna daya samfurin rahoto sigogi
Danna wani layi na ƙwayoyin da ke nuna shafi don nuna wani samfurin rahoto rahoto sigogi, Figure 6.15.
6 Kulawa da Kulawa
6.1 Tsabtaccen Gida
Kula da dakin gwaje-gwaje tsabtace da dakin gwaje-gwaje muhalli, yin a kai a kai tsabtace dakin gwaje-gwaje, kauce wa daban-daban madubi da ƙura rufe tasirin haske ta hanyar ** makamashi. Bayan gwajin, gwajin kayan aiki dole ne a shirya tsabta, da acid abubuwa daga kayan aiki da kuma kiyaye kayan aiki gida zafi. Don kauce wa acid gas lalata na'urorin gani, molding.
6.2 Bincike na yau da kullun
6.2.1 Bincika sharar ruwa bututun ba sa sharar ruwa surface nutsar da sharar ruwa bututun da kuma zubar da sharar ruwa a kan lokaci.
6.2.1 sharar ruwa bututun accumulated ruwa ya isa a kasa da spray drum zai sa a lokacin ma'auni sosai m, don haka a kowane lokaci bincika ko sharar ruwa bututun da aka bude, lokaci-lokaci zubar da sharar ruwa.
6.2.1 a kai a kai dubawa na acetylene gas hanyoyin don kauce wa bututun hanyoyin tsufa samar da gas leakage lamarin, hadari.
6.2.1 bincika gas hanya a kai a kai, bayan kowane canza acetylene gas cylinder tabbatar da ** gwajin leakage. Ta amfani da ruwa kamar ruwan sabulu da zai iya bincika yanayin leakage a duk hanyoyin dubawa, duba ko akwai kumfa da aka samar, da kuma yanke hukunci idan ya leak. Lura bincika na yau da kullun ko akwai gas leakage, duba hanyar bincike don binciken acetylene.
6.3 Haske
FEA biyar abubuwa analyzer karɓar baƙi a cikin dogon lokaci ba tare da amfani, don Allah riƙe kowane * biyu makonni a lokacin da kayan aikin bude da pre-dumama a kan layi na 1 ~ 2 hours. Don tsawaita amfani da shekaru. Ba za a iya amfani da hasken hasken na dogon lokaci ba, ba za a iya amfani da shi ba saboda zubar da iskar gas, sassan da sauran dalilai, ba za a iya ƙone shi ba. Saboda haka ya kamata a yi amfani da hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken hasken has
6.4 Tsarin gani
Kayan gani na hanyar haske na waje sau da yawa suna tsabta, yawanci * ƙananan tsabtace sau ɗaya a shekara. Idan akwai ƙura a kan gani abubuwa, akwai share madubi takarda tsabtace; Idan an yi amfani da gurɓataccen mai a kan kayan gani ko kuma an yi amfani da gurɓataccen mai a lokacin ƙididdigar samfurin maganin, za a iya gwada shi da garbage da aka wanke da bushewa a cikin haɗin ethanol da ether (1: 1), sa'an nan kuma ruwan da aka yi amfani da shi ya wanke sabulu, sa'an nan kuma a bushe shi da kwallon kunya. A lokacin tsaftacewa, kashe hannunsa don gogewa da kayan ƙarfe ko taɓa madubi.
6.5 atomizer tsarin
Kowane bincike * da aka kammala, musamman bayan bincike da yawa matattarar ko Strong acid samfurin, nan da nan spray da dama mintuna na ruwa distilled don hana sprayer cylinder da ƙonewa kai ne gurbataccen ko zazi. Bayan ƙonewa, a saman dukan ramin mai ƙona ya kamata a sami wuta mai launin shuɗi mai ƙona daidai-daidai. Idan kwalliyar wuta ta bayyana a tsakiyar rami, yana da zane-zane, yana nuna cewa akwai datti ko hatsi a sama da ƙonawar kai, a wannan lokacin ana buƙatar tsaftacewa, hanyar tsaftacewa ita ce haɗin iska, rufe acetylene a ƙarƙashin yanayin, don saka takarda mai tacewa a cikin ƙonawa; Kamar ** Bad za a iya cire ƙonewa kai wanke da m gashi burshe; Kamar yadda aka samar da ƙwayoyin narkewa, za a iya amfani da takarda mai ƙarfe mai ƙarfe ko ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin ƙwayoyin
6.6 Air hanyar tsarin
An haramta amfani da jan ƙarfe da azurfa a cikin bututun gas na acetylene, kuma an haramta man fetur. Lokacin gwajin mafita na jan ƙarfe ko azurfa mai yawa, ya kamata a wanke shi sau da yawa ta amfani da ruwan de-ion. Don sau da yawa watsa da ruwa da aka tara na iska mai matsawa mai rarraba ruwa, don hana ruwa shiga gas mai amfani. Lokacin da aka kammala ma'auni na kayan aiki, ya kamata a kashe acetylene gas da farko, sa'an nan kuma kashe gas bawul bayan wuta a kan burner, ** kashe iska kwamfuta.
6.7 Sauya tubu na inshora a kai a kai.
Idan ba za a iya magance wasu matsalolin da aka samu ba a lokacin amfani da samfurin, don Allah tuntuɓi sashin sabis na bayan tallace-tallace na Daqing Nisheng Instrument Manufacturing Co., Ltd., waya: 0459-8186000.
Annex 1 Gwajin aikin kayan aiki (don kamfanonin samarwa)
0 al'ada aiki yanayi
Kayan aiki yanayin ya kamata sadu da:
a) yanayin zafin jiki 15 ℃ ~ 30 ℃;
b) dangi zafi ba fiye da 75%;
c) girgizawa da kuma electromagnetic tsangwama da ba tasiri amfani da kayan aiki;
d) babu lalata gas a cikin gida, da kyau iska na'urori;
e) Wutar lantarki: ƙarfin lantarki 220V ± 22V, mita 50Hz ± 1Hz.
1 auna halin yanzu haske ƙarfin lantarki
1.1 Ma'anar halin yanzu haske ƙarfin lantarki: lambar da kuma adadin haske lokacin da babu haske shigarwa. Yanzu haske ƙarfin lantarki ya shafi linearity da kuma m na misali aiki curve. Lambobi da adadin haske a lokacin da babu haske shigar da aka ayyana a matsayin scattered haske.
1.2 Hanyar auna halin yanzu haske ƙarfin lantarki: rufe a cikin haske, danna kan saman menu "aiki auna", auna lokaci fiye da 200 seconds. Danna "" button a cikin don fara auna halin yanzu haske ƙarfin lantarki. Duba hotuna na 1.2 da 1.2. Danna a kan button don lissafin halin yanzu lantarkin lantarki.
2 m amo fadi
2.1 Ma'anar tsayayye amo fadi: tsayayye amo fadi Hb ne sau 3 na misali karkatarwa S na lambar ** a karkashin babu kunnawa jihar.
2.2 Tsayayye amo fadi lissafi formula: Hb = 3 × S
3 Wuta amo fadi
3.1 Ma'anar wuta hayaniya fadi: wuta hayaniya fadi Hb ne sau 3 na misali karkatarwa S na lambar ** a cikin yanayin ƙonewa.
3.2 Calculation formula na wuta amo fadi: Hb = 3 × S
3.3 hanyar ma'auni na wuta amo fadi: danna kan saman matakin "aikin ma'auni" menu, ma'auni lokaci fiye da 200 seconds, a cikin yanayin ƙonewa, danna
4 Kuskuren layi E
4.1 Ma'anar kuskuren layi E: E = [Σ (100 × dC / C)]/3
4.2 lissafi Formula: Parabolic komawa nazarin: dC = |c × A × A + b × A + a - C |
C = c × A × A + b × A + a
Tsarin:
c, b, a -- daidaitaccen abubuwa.
A ---- absorption.
5 ƙwarewa
5.1 Ma'anar hankali: shi ne matsakaicin ma'auni na absorbance na daidaitaccen bayani na 3 sau 7 a jere.
5.2 Lissafin ƙwarewa: ƙwarewa = 5 55.2 As / 7
Tsarin:
As ---- No. 3 misali bayani absorption.
6 Maimaitawa
6.1 Ma'anar maimaitawa: shi ne dangane da daidaitaccen karkatarwa na RSD na auna absorbance na daidaitaccen bayani na No. 3 sau bakwai a jere.
6.2 Maimaita lissafi formula
Tsarin:
A ---- No. 3 misali bayani absorption.
7 Bayani iyaka
7.1 Ma'anar ƙuntatawa DL: shi ne matattarar da aka gwada daidai da asali fadin Hb.
7.2 lissafi formula don gano iyaka DL: DL = Hb × Cs / A
Tsarin:
Cs ---- matattarar daidaitaccen bayani na 3;
A ---- No. 3 misali bayani absorption;
Hb --- amo fadi.
8 siffofin mayar da hankali
Ma'anar siffofin matattarar: shi ne matattarar da aka auna daidai da 99% na haske (absorbance A = 0.0043648).
lissafin formula na halaye mayar da hankali: halaye mayar da hankali = 0.0043648 × Cs / A
Tsarin:
Cs ---- matattarar daidaitaccen bayani na 3,
A ---- No. 3 misali bayani absorption.
9 Hanyoyin auna alamun aiki
9.3 ƙonewa
9.3.1 Man fetur-free iska kwamfuta: Tabbatar da cewa iska hanyar haɗi ne mai kyau, daidaita da kwararar daidaitawa bawul na iska kwamfuta a saba da agogo agogo zuwa **, bude iska kwamfuta wutar lantarki, daidaita da kwararar bawul a saba da agogo agogo, sa iska matsin lamba ne 0.23Mpa.
9.3.2 acetylene ** na'urar: bude bawul na acetylene karfe kwalba, daya matsin lamba mita ba zai iya kasa da 0.4MPa, daidaita biyu matsin lamba mita, tabbatar da cewa acetylene matsin lamba ne 0.03Mpa. Danna *** button yayin da aka ƙona kai tare da wuta lighter. Daidaita acetylene kusa da ƙonawa kai tare da iska sarrafa bawul, lura da wuta kwanciyar hankali, da launi a tan dakatar. Ma'auni suction hakkin kimanin 6ml / min.
Lura: Idan acetylene matsin lamba ba a cikin aiki kewayon (0.02Mpa-0.08 Mpa), to, acetylene ** na'urar ta atomatik kashe iska tushen, aiki nuna alama fitila walƙiya, ƙararrawa sauti, ** nuna alama haske. Re-daidaita acetylene gas tushen ne 0.03Mpa, danna [** Button] lokaci guda kunna ƙonawa kai da wuta lighter.
Annex 2 reagent shirya
1 Tsarin daidaitaccen bayani na ajiya (tsarawa a cikin kabatin iska)
1.1 2400 mg / L calcium misali ajiya mafita: auna 5.9934g na benchmark calcium carbonate [CaCO3] bushewa 3h a 105-110 digiri, a cikin kwalba 1000mL karfin, a hankali ƙara 20mL hydrochloric acid, ƙara 200mL ruwa, ruwan wanka dumama * narkewa, kwanciyar hankali.
1.2 300mg / L jan ƙarfe misali ajiya bayani: auna 0.3000g high tsabtace jan ƙarfe [Cu] ƙara * 50ml kokarin, ƙara 10ml tsabtace ruwa, a hankali ƙara 10ml nitric acid, wutar lantarki murya a sama da microboiling * launi m. Ƙara 20mL ruwa, cire, sanyaya, motsa a cikin kwalban 1000mL na ƙarfin aiki, daidaita.
1.3 1200 mg / L magnesium misali ajiya mafita: auna 1.2000g high tsabtace magnesium [Mg] ƙara * 50ml kokarin, ƙara 10ml tsabtace ruwa, a hankali ƙara 10ml hydrochloric acid, wuta microboiling a sama murya * launi-launi m. Ƙara 30mL ruwa, cire, sanyaya, motsa a cikin kwalban 1000mL na ƙarfin aiki, daidaita.
1.4 15000mg / L Iron misali ajiya bayani: auna 1.5000g high tsabtace baƙin ƙarfe [Fe] ƙara * 100mL kokarin, ƙara 10mL tsabtace ruwa, a hankali ƙara 10mL nitric acid, wuta microboiling sama da tanda, a hankali drop ƙara 10mL hydrochloric acid taimakon narkewa, * launi m. Ƙara 50mL ruwa, cire, sanyaya, motsa a cikin kwalban 100mL, ƙara ruwa mai tsabtace 600mL.
1.5 450mg / L zinc misali ajiya bayani: auna 0.4500g high tsabtace zinc [Zn] ƙara * 50ml kokarin, ƙara 10ml tsabtace ruwa, a hankali ƙara 10ml hydrochloric acid, wutar lantarki a saman da wuta micro tafiya * launi-free m. Ƙara 100mL ruwa, cire, sanyaya, motsa a cikin kwalban 1000mL na ƙarfin aiki, daidaita.
2 Biyar abubuwa daidaitaccen ajiya bayani (48mg / L Calcium Ca, 6.00mg / L jan ƙarfe Cu, 24mg / L magnesium Mg, 300mg / L Iron Fe, 9.00mg / L Zinc Zn): An ƙara 2400 mg / L calcium daidaitaccen ajiya bayani, 300mg / L jan ƙarfe daidaitaccen ajiya bayani, 1200 mg / L magnesium daidaitaccen ajiya bayani 10.00mL, 15000mg / L baƙin ƙarfe daidaitaccen ajiya bayani da 450mg / L zinc daidaitaccen ajiya bayani da 10.00mL.
3 Standard jerin mafita
3.0 0 ** mafita (cikakken jini biyar abubuwa ** reagent): suck 5.00mL hydrochloric acid ƙara * 1000mL damar kwalba, da lafiya. An rarraba shi a cikin kwalban filastik na 50ml. An rarraba shi a cikin 1.00mL roba centrifugal bututu, 1.000mL a kowace kwalba. 100 na 1 akwati. Cikakken jini mai rarrabuwa.
3.1 No. 1 misali bayani (0.800mg / L Calcium Ca, 0.100mg / L jan ƙarfe Cu, 0.40mg / L magnesium Mg, 5.00mg / L Iron Fe, 0.150mg / L Zinc Zn): sha 25.00mL biyar abubuwa misali ajiya bayani, ƙara * 2000mL damar kwalba, ƙara 10.0mL hydrochloric acid, daidaitawa. An rarraba shi a cikin kwalban filastik na 50ml, kowane kwalba ba kasa da 50ml ba.
3.2 No. 2 misali bayani (1.60mg / L Calcium Ca, 0.200mg / L jan ƙarfe Cu, 0.80mg / L magnesium Mg, 10.00mg / L Iron Fe, 0.30mg / L Zinc Zn): sha 25.00mL biyar abubuwa misali ajiya bayani, ƙara * 1000mL damar kwalba, ƙara 5.0mL hydrochloric acid, daidaitawa. An rarraba shi a cikin kwalban filastik na 50ml, kowane kwalba ba kasa da 50ml ba.
3.3 No. 3 misali bayani (2.40mg / L Calcium Ca, 0.300mg / L jan ƙarfe Cu, 1.20mg / L magnesium Mg, 15.00mg / L Iron Fe, 0.450mg / L Zinc Zn): sha 25.00mL biyar abubuwa misali ajiya bayani, ƙara * 500mL damar kwalba, ƙara 2.50mL hydrochloric acid, daidaitawa. An rarraba shi a cikin kwalban filastik na 50ml, kowane kwalba ba kasa da 50ml ba.
4 Standard mafita (samar da kamfanoni)
4.1 240mg / L calcium misali bayani: suck 2400 mg / L calcium misali ajiya bayani 10.00mL ƙara * 100mL damar kwalba, da kwanciyar.
4.2 30mg / L jan ƙarfe misali bayani: suck 300mg / L jan ƙarfe misali ajiya bayani 10.00mL ƙara * 100mL damar kwalba, da kwanciyar.
4.3 120mg / L magnesium daidaitaccen bayani: suck a cikin 1200mg / L magnesium daidaitaccen ajiya bayani 10.00mL ƙara * 100mL damar kwalba, daidaitawa.
4.4 1500mg / L baƙin ƙarfe misali bayani: suck a cikin 15000 mg / L baƙin ƙarfe misali ajiya bayani 10.00mL ƙara * 100mL damar kwalba, da kuma sanya.
4.5 45mg / L zinc misali bayani: suck 450mg / L zinc misali ajiya bayani 10.00mL ƙara * 100mL damar kwalba, da kwanciyar.
5 Standard aikace-aikace ruwa (samar da kamfanoni) Hanyar tsarawa 1:
5.1 2.40mg / L Calcium daidaitaccen aikace-aikace mafita: suck 240mg / L Calcium daidaitaccen mafita 10.00mL ƙara * 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, daidaitawa.
5.2 0.300mg / L jan ƙarfe misali aikace-aikace mafita: suck 30mg / L jan ƙarfe misali mafita 10.00mL ƙara * 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, kwanciya.
5.3 1.20mg / L magnesium daidaitaccen aikace-aikace mafita: suck 120mg / L magnesium daidaitaccen mafita 10.00mL ƙara * 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, kwanciyar hankali.
5.4 15.00mg / L Iron misali aikace-aikace mafita: shan 1500mg / L Iron misali mafita 10.00mL ƙara 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, daidaitawa.
5.5 0.450mg / L zinc misali aikace-aikace mafita: suck 45mg / L zinc misali mafita 10.00mL ƙara * 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, daidaitawa.
5 Standard aikace-aikace ruwa (samar da kamfanoni) Hanyar tsarawa 2:
5.1 2.40mg / L Calcium daidaitaccen aikace-aikace mafita: suck 2400mg / L Calcium daidaitaccen mafita 1.00mL ƙara * 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, daidaitawa.
5.2 0.300mg / L jan ƙarfe misali aikace-aikace mafita: suck 300mg / L jan ƙarfe misali mafita 1.00mL ƙara * 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, kwanciya.
5.3 1.20mg / L magnesium daidaitaccen aikace-aikace mafita: suck 120mg / L magnesium daidaitaccen mafita 1.00mL ƙara * 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, settling.
5.4 15.00mg / L Iron misali aikace-aikace mafita: suck 1500mg / L Iron misali mafita 1.00mL ƙara 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, daidaitawa.
5.5 0.450mg / L zinc misali aikace-aikace mafita: suck 45mg / L zinc misali mafita 1.00mL ƙara * 1000mL damar kwalba, ƙara 5.00mL hydrochloric acid, daidaitawa.
Annex 3 Biyar abubuwa Standard ajiya bayani Easy formulation
(An tsara shi a cikin kabatin iska)
Da farko ta amfani da aikace-aikacen ruwa na kayan aikin da aka tsara don tantance calcium carbonate [CaCO3], jan ƙarfe mai tsabta [Cu], magnesium mai tsabta [Mg], ƙarfe mai tsabta [Fe] da zinc mai tsabta [Zn] ba tare da tsangwama ba, ana amfani da corrugated don tsara daidaitaccen bayani na asali na abubuwa biyar.
6 Original biyar abubuwa misali ajiya bayani (2400 mg / L calcium-300mg / L jan ƙarfe-1200 mg / L magnesium-15000mg / L baƙin ƙarfe-450mg / L zinc)
Ka auna 5.9934g na calcium carbonate [CaCO3] da aka bushe a 105-110 digiri a 3h a cikin kwalban ƙarfin * 1000mL, ka ƙara 0.3000g mai tsabta jan ƙarfe [Cu], ka ƙara 1.2000g mai tsabta magnesium [Mg], ka ƙara 15.000g mai tsabta baƙin ƙarfe [Fe], ka ƙara 0.4500g mai tsabta zinc [Zn]. Ƙara ruwa 20mL, sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin sauƙin Capacity kwalba sa a kan tafiya ruwa wanka na sa'a daya, shake na minti daya, ƙara ruwa * kimanin 800mL, sanyaya, daidaitawa. Wannan ruwa 10.00mL kunshe a cikin 1 ampere kwalba ** ajiye.
2 Biyar abubuwa misali ajiya bayani (48mg / L Calcium Ca, 6.00mg / L jan ƙarfe Cu, 24mg / L magnesium Mg, 300mg / L Iron Fe, 9.00mg / L zinc Zn): suck asali biyar abubuwa misali ajiya bayani 10.00mL ƙara * 500mL damar kwalba, laying.
Annex 7 Shirya kayan aikin gilashi na Annex 2 da Annex 3 (don kowane kwalba)
7.1 Kofi da Pipeline
|
lambar |
Sunan |
adadin |
lambar |
Sunan |
adadin |
lambar |
Sunan |
adadin |
|
1 |
50ml kokarin |
4 |
8 |
80 × 80 sulfuric takarda |
100 |
15 |
Tape mai haske |
1 takardar |
|
2 |
100ml Kofi |
1 |
9 |
reagent rack |
1 daga |
16 |
kwalba |
1 daga |
|
3 |
10ml Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular |
10 |
10 |
500W daidaitaccen wutar lantarki |
1 daga |
17 |
sucking Ball |
1 daga |
|
4 |
25ml Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular Tubular |
1 |
11 |
tsawon 200 diamita 10 gilashin sanduna |
1 daga |
18 |
Label takarda |
3 kuma |
|
5 |
10ml Mai Tsara |
10 |
12 |
10L ƙasa bakin kwalba |
1 daga |
19 |
Ruwa kwalba |
1 daga |
|
6 |
50ml filastik kwalba |
20 daga |
13 |
Deionized ruwa (20L roba kwandon) |
20L |
20 |
Rubber hannu |
1 biya |
|
7 |
kananan shears |
1 daga |
14 |
takarda tacewa |
1 akwati |
21 |
Nazarin sikelin |
1 daga |
7.2 Capacity kwalba 20 da Labels
|
Sunan |
adadin |
Labels |
|
|
1000ml damar kwalba
|
13
|
1.1 2400 mg / L calcium misali ajiya mafita |
6 Original biyar abubuwa Standard ajiya bayani
2400 mg / L na calcium
300mg / L jan ƙarfe
1000 mg / L 镁
15000mg / L ƙarfe
450mg / L ƙarfe)
|
|
1.2 300mg / L jan ƙarfe misali ajiya mafita |
|||
|
1.3 1200 mg / L Magnesium daidaitaccen ajiya mafita |
|||
|
1.5 450mg / L Zinc misali ajiya mafita |
|||
|
Shirya biyar abubuwa Standard ajiya bayani |
|||
|
No. 0 ** mafita |
|||
|
No. 2 daidaitaccen bayani |
|
||
|
5.1 2.40mg / L Calcium misali aikace-aikace mafita |
|
||
|
5.2 0.300mg / L jan ƙarfe misali aikace-aikace mafita |
|
||
|
5.3 1.20mg / L magnesium misali aikace-aikace mafita |
|
||
|
5.4 15.00mg / L Iron misali aikace-aikace mafita |
|
||
|
5.5 0.450mg / L Zinc misali aikace-aikace mafita |
|
||
|
500ml damar kwalba |
1 |
No. 3 daidaitaccen bayani |
|
|
2000ml damar kwalba |
1 |
No. 1 daidaitaccen bayani |
|
|
100ml ƙarfin kwalba
|
6
|
1.4 15000mg / L Iron misali ajiya mafita |
|
|
4.1 240mg / L calcium misali mafita |
|
||
|
4.2 30mg / L jan ƙarfe misali mafita |
|
||
|
4.3 120mg / L Magnesium daidaitaccen mafita |
|
||
|
4.4 1500mg / L Iron misali mafita |
|
||
|
4.5 45mg / L Zinc daidaitaccen mafita |
|
1.7 Biyar abubuwa spectrum bayanai
Table 1.8.1 Biyar abubuwa spectrum bayanai
|
Abubuwan |
Calcium Ca |
jan ƙarfe Cu |
Magnesium Mg |
Iron Fe |
Zinc Zn |
|
Yanayin nm |
422.67 |
324.75 |
285.21 |
252.3 lokaci m layi |
213.86 |
|
atomic nauyin |
40.08 |
63.546 |
24.305 |
55.847 |
65.38 |
|
Matsayi |
Kalsiyamu carbonate |
High tsabtace jan ƙarfe |
magnesium oxide |
Ammonium sulfate na ƙarfe |
Babban tsabtace zinc [Zn] |
|
kwayoyin formula |
CaCO3 |
[Su] |
MgO |
[FeSO4·(NH4)2SO4·6H2O] |
|
|
Matsayin nauyin kwayoyin |
100.09 |
63.546 |
40.304 |
392.1308 |
65.38 |
|
Spacebar nisan nm |
30 |
200 |
200 |
200 |
200 |
1.9 Raster bayanai
Roland zagaye diamita = 224.000mm, line adadin / mm = 1200, shiga kusurwa = 0, spectrum bayanai duba tebur 1.9. Duba hoto na 1.9.
Tebur 1.9 Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan Bayanan
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